2016年6月30日星期四

Hydrolysis device,Double wall glass reactor

1, Hydrolysis reactor (10L ,20L,50L,100L)



Function:
Single layer glass reactor is an equipment which is a collaboration of vacuum state,
distillation, reflux, stirring, oil/water heating, heating mantle. It can do all kinds of biochemical reactions and synthesis reactions at a constant temperature condition. 
It is also a closed system on the whole. 
Circulating water vacuum pump can pump into the reactor sorts of liquids and gases. Thereflux or distillation is possible under different temperature state.
The single layer glass reactor has water/oil heating bath or heating mantle 
itself. Water/oil bath temperature is digital display,which can meet constant 
temperature state,fast temp. rising, accurate controllers.1-50L is circular and more 
than 50L is cylinder. After heating we can add the cooling coil in the tank to cool thematerial in short time




2nd type.   Double Jacket Reactor







2016年4月23日星期六

BMK precursors and BMK(Phenylacetone), Cas 103-79-7

BMK precursors and BMK

We ship the products from Netherlands/Belgium warehouses for you now.
Please contact us for Ciphr or Sky ecc to talk.

How to convert BMK powder to oil?(Below is just a general description of hydrolysis process, you may still need to contact us if you cannot get oil properly.)
1,1kg powder mix with 1kg warm water (around 80 degrees).
2, put in 1kg hydrochloric acid (HCL 37%) and you will see bubble generated.
3,Stirring the mixture for one hour and then stop.
4,After one more hour you will get oil layer in light yellow color.
5,Use separate funnel to retrieve oil. 

Contact BMK precursor (Cas 4468-48-8) Supplier

Email : chemjonny@protonmail.com
Wickr : chemjonny

Phenylacetone Specification

The IUPAC name of Phenylacetone is 1-phenylpropan-2-one. With the CAS registry number 103-79-7, it is also named as Benzyl methyl ketone. The product's categories are Acetylgroup; Pharmaceutical Intermediates. It is colorless to pale yellow liquid which is insoluble in water, soluble in alcohol, acetone, benzene and other organic solvents and stable in normal temperature and pressure. Additionally, this chemical should be sealed in the container and stored in the cool and dry place.

The other characteristics of Phenylacetone can be summarized as:(1)ACD/LogP: 1.44; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): 1.44; (4)ACD/LogD (pH 7.4): 1.44; (5)#H bond acceptors: 1; (6)#H bond donors: 0; (7)#Freely Rotating Bonds: 2; (8)Index of Refraction: 1.507; (9)Molar Refractivity: 40.46 cm3; (10)Molar Volume: 135.8 cm3; (11)Polarizability: 16.04×10-24 cm3; (12)Surface Tension: 34.2 dyne/cm; (13)Flash Point: 87.5 °C; (14)Enthalpy of Vaporization: 45.03 kJ/mol; (15)Boiling Point: 214 °C at 760 mmHg; (16)Vapour Pressure: 0.159 mmHg at 25°C; (17)Rotatable Bond Count: 2; (18)Tautomer Count: 3; (19)Exact Mass: 134.073165; (20)MonoIsotopic Mass: 134.073165; (21)Topological Polar Surface Area: 17.1; (22)Heavy Atom Count: 10; (23)Complexity: 112.
Preparation of Phenylacetone: It can be obtained by many methods. A conceptually simple example of phenylacetone organic synthesis is the Friedel-Crafts alkylation of benzene with chloroacetone.
Uses of Phenylacetone: It is used in the manufacture of methamphetamine and amphetamine. It is also used as intermediate of rodenticide diphacinone and chlorophacinone. In addition, this chemical can be used in many organic synthesis. For example: it can react with 2-chloro-acetamide to get 5-methyl-4-phenyl-1,3-dihydro-pyrrol-2-one. This reaction needs reagent t-BuOK and solvent dimethylsulfoxide at temperature of 80 °C. The reaction time is 3 hours. The yield is 35%.
People can use the following data to convert to the molecule structure. 1. SMILES:O=C(C)Cc1ccccc1
2. InChI:InChI=1/C9H10O/c1-8(10)7-9-5-3-2-4-6-9/h2-6H,7H2,1H3
3. InChIKey:QCCDLTOVEPVEJK-UHFFFAOYAG

PMK oil,Piperonyl Methyl Ketone,Cas 4676-39-5

PMK cas 4676-39-5
We ship the products in Netherlands/Belgium.
Please contact us for Ciphr or Sky ecc to talk.

How to convert pmk powder to oil?(Below is just a general description of hydrolysis process, you may still need to contact us if you cannot get oil properly.)
1,1kg powder mix with 1kg warm water (around 80 degrees).
2, put in 1kg hydrochloric acid (HCL 37%) and you will see bubble generated.
3,Stirring the mixture for one hour and then stop.
4,After one more hour you will get oil layer in light yellow color.
5,Use separatory funnel to retrieve oil. 
6,To purify oil. Extra by DCM-->Wash with NaOH-->Distillation .

Contact PMK (Cas 4676-39-5) Supplier

Email : chemjonny@protonmail.com
Wickr : chemjonny

PMK related products

  • PMK Glycidate(Cas 13605-48-6)
  • PIPERONYL METHYL KETONE(Cas 4676-39-5)
  • Alpha-acetylphenylacetonitrile (Cas 4468-48-8)
  • Benzeneacetic acid(Cas 16648-44-5)
  • alpha-Acetylbenzeneacetic acid(Cas 4433-88-9)
  • Phenylacetone(Cas 103-79-7)
We provide raw materials, intermediates,catalyst as well as final products. We also support with tools and technique consulting.Please feel free to contact.

PMK oil,Piperonyl Methyl Ketone,Cas 4676-39-5

PMK cas 4676-39-5
We ship the products from Netherlands/Belgium warehouses for you now.
Please contact us for BB PGP or ECC ID(BB Sky Phone) to talk.

How to convert pmk powder to oil?(Below is just a general description of hydrolysis process, you may still need to contact us if you cannot get oil properly.)
1,1kg powder mix with 1kg warm water (around 80 degrees).
2, put in 1kg hydrochloric acid (HCL 37%) and you will see bubble generated.
3,Stirring the mixture for one hour and then stop.
4,After one more hour you will get oil layer in light yellow color.
5,Use separatory funnel to retrieve oil. 
6,To purify oil. Extra by DCM-->Wash with NaOH-->Distillation .

Contact PMK (Cas 4676-39-5) Supplier

Email : chemjonny@openmailbox.org
Wickr : chemjonny

PMK related products

We provide raw materials, intermediates,catalyst as well as final products. We also support with tools and technique consulting.Please feel free to contact.

PMK Glycidate,PMK powder, cas 13605-48-6

PMK Glycidate Cas 13605-48-6

Product Name: Methyl 3-[3’,4’-(methylenedioxy)phenyl]-2-methyl glycidate
We ship the products in Netherlands/Belgium
Please contact us for ciphr or Sky ECC to talk.
The powder gives a high yield(75%) of PMK oil . And the process of converting powder to oil is quite simple and easy, please contact to get recipe.

Contact us to get PMK Glycidate (cas 13605-48-6).

  • Email : chemjonny@protonmail.com
  • Wickr : chemjonny
How to convert powder to oil?(Below is just a general description of hydrolysis process, you may still need to contact us if you cannot get oil properly.)
1,1kg powder mix with 1kg warm water (around 80 degrees).
2, put in 1kg hydrochloric acid (HCL 37%) and you will see bubble generated.
3,Stirring the mixture for one hour and then stop.
4,After one more hour you will get oil layer in light yellow color.
5,Use separatory funnel to retrieve oil. 

Related products

PMK precursors and PMK
(1), 3,4-MDP-2-P intermediate;PMK Glycidate;PMK powder  Cas no:13605-48-6
(2),Piperonyl methyl ketone / PMK Oil / MDP2P  CAS No.: 4676-39-5

BMK precursors and BMK

(1),Alpha-acetylphenylacetonitrile (Cas 4468-48-8)
(2),Benzeneacetic acid, a-acetyl-, methyl ester (Cas 16648-44-5)
(3),3-oxo-2-phenylbutanoic acid ; alpha-Acetylbenzeneacetic acid (Cas 4433-88-9)

【Synonyms of PMK Glycidate,cas 13605-48-6】

PMK intermediate;
3,4-MDP-2-P intermediate;
Appearance: yellow powder;
Assay: 98%min;
Package: 25KG/Drum;
Usage:pharmaceutical intermediate, PMK intermediate, 3,4-MDP-2-P intermediate;